Yıldırım Uçan, GamzeAtalmış, Gamze2019-12-022019-12-0220142014-06Atalmış, G. (2014). Substitüe salen komplekslerinin sentezi. (Yüksek Lisans Tezi) Niğde Üniversitesi, Fen Bilimleri Enstitüsü, Niğdehttps://hdl.handle.net/11480/7389Bu çalışmada çıkış maddesi olarak 2,4-dihidroksi benzaldehit kullanıldı. 2,4-dihidroksi benzaldehit ile 1,2-fenilendiaminden reaksiyonundan; N,N'-Bis(2,4-dihidroksi benziliden)-fenilen-1,2-diamin sentezlendi. N,N'-Bis(2,4-dihidroksi benziliden)-fenilen-1,2-diamin ile N-(1-Pirenil) kloroasetamit'ten yeni bir Schiff baz ligandı sentezlendi. Schiff Bazının Ni(II), Cu(II), Co(II), Zn(II) ve Hg(II) asetatları ile beş metal kompleksi sentezlendi. Sentezlenen Sekiz yeni bileşiğin yapıları; Magnetik Susseptibilite, Molar İletkenlik, Elementel Analiz, FT-IR, 1H-NMR, UV-Vis,Floresans Spektroskopisive TGA yöntemleriyle aydınlatılmaya çalışıldı.In this study 2,4-dihydroxy benzaldehyde was used as a starting meterial. N,N'-Bis(2,4-dihydroxybenzylidene)-phenylene-1,2-diamine was synthesized by using 2,4-dihydroxy benzaldehyde and 1,2-phenylenediamine. A new Schiff base ligand was synthesized by reaction with N,N'-Bis(2,4-dihydroxybenzylidene)-phenylene-1,2-diamine and N-(1-pyrenyl)chloroacetamide. Thecomplexes of Schiff base were synthesized by Ni(II), Cu(II), Co(II), Zn(II) and Hg(II) acetat salts. As a conclusion of above work, new one ligand and their complexes were characterized by FT-IR, 1H NMR, UV-Vis, TGA ve Magnetic Susceptibility, fluorescence spectroscopy, elementary analysis.trinfo:eu-repo/semantics/openAccessSchiff BazıFloresans Spektroskopisi1-AminoprenN-(1-Pirenil)-2-kloroasetamitMetal KomplekslerSchiffbaseFluorescencespectroscopy1-AminopyreneN-(1-pyrenyl)-2-chloroacetamideMetal ComplexesMaster Thesis372600