Yildirim S.Pekacar A.I.Uçan M.2019-08-012019-08-0120030094-5714https://dx.doi.org/10.1081/SIM-120021654https://hdl.handle.net/11480/1338anti-2-Naphthylchloroglyoxime has been synthesized by chlorination of anti-2-naphthylglyoxime. Reaction with aryl-or arylalkylamines in EtOH between 15°C and 20°C gives unsymmetrical vic-dioximes, namely, anilino-2-naphthylglyoxime (L1H2), benzylamino-2-naphthylglyoxime (L2H2), p-toluidino-2-naphthylglyoxime (L3H2) 1-naphthylamino-2-naphthylglyoxime (L4H2). The Ni(II) and Cu(II) complexes of these ligands are square-planar while the Co(II) complexes are octahedral with water molecules as axial ligands. 1H NMR, IR and elemental analyses data of the complexes and ligands are discussed.eninfo:eu-repo/semantics/closedAccessArticle33587388210.1081/SIM-1200216542-s2.0-0038449332N/AWOS:000183374700010Q4