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Synthesis and characterization of some vic-dioxime and its mononuclear complexes
(MAIK NAUKA/INTERPERIODICA/SPRINGER, 2007) Uysal, S.; Coskun, A.; Koc, Z. E.; Ucan, M.; Ucan, H. I.
In this study, acetophenone is used as a basis substance. omega-Isonitrosoacetophenone has been synthesized from nitrosyl with amyl nitrite of acetophenone in the presence of sodium ethoxide. Subsequently, anti-phenylglyoxime has been prepared by reacting omega-isonitrosoacetophenone with hydroxylamine and sodium acetate in a ethanolic media. Chlorophenylglyoxime has been obtained from reaction with chlorine gases. Then, three aminophenylglyoxime (ligands) have been prepared by the reaction of chlorophenylglyoxime and the corresponding amines. The Ni(II), Co(II), and Cu(II) complexes with BF2+-bridge of anilinophenylglyoxime and 2,4-dimethylanilinophenylglyoxime were prepared. Then polymeric metal complexes with BF2+-bridge of dopamiophenylglyoxime were prepared. Their structures were identified by FT-IR, H-1 NMR, and ICP-AES spectral data, elemental analysis and magnetic measurements.
Synthesis and characterization of some vic-dioxime and its mononuclear complexes (vol 33, pg 351, 2007)
(MAIK NAUKA/INTERPERIODICA/SPRINGER, 2007) Uysal, S.; Coskun, A.; Koc, Z. E.; Ucan, M.; Ucan, H. I.
[Abstract Not Available]