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Öğe A study on thermoluminescence behaviour of Eu doped LaB3O6 irradiated with beta particles(Pergamon-Elsevier Science Ltd, 2020) Halefoglu, Y. Z.; Oglakci, M.; Portakal, Z. G.; Akca, S.; Souadi, G. O.; Canimoglu, A.; Topaksu, M.Lantanium triborate (LaB3O6) samples doped with Eu3+ ions are synthesized via combustion route. This study primarily reports the thermoluminescence (TL) behaviour of LaB3O6 host. X-ray diffraction (XRD) pattern reveals that LaB3O6 exhibits a single phase matched with JCPDS card 98-002-3609. Dose response, reusability and trap parameters of TL glow curves are evaluated to clearly reveal the TL features. The results show that the peak positions of TL glow curves are affected by varying the concentration of Eu. The experimental results obtained from the dose-response of LaB3O6:Eu3+ (1%) which has given high TL intensity reveal that the intensity of TL given by the total area under glow curves shows a good linearity (b = 0.997) up to 20 Gy. In addition, the minimum detectable dose (MDD) value has been calculated as 1.45 mGy with a standard deviation of 0.8%. Main TL peak maxima is observed around 197 degrees C with heating rate (HR) of 2 degrees Cs-1. An anomalous HR effect is observed for this peak in the range of 0.5-20 degrees Cs-1 with beta dose of 5 Gy. To find the overlapping peak numbers and determine the kinetic parameters of the main peak of LaB3O6:Eu3+ (1%), Initial Rise (IR) method using T-m - T-stop experiment and CGCD analysis have been performed for HRs of 0.5 and 2 degrees Cs-1. It can be said that the results of the methods are in good agreement when same trap numbers (at least eight separate peaks for both) and close energy values are taken into consideration. Deconvolution procedure of LaB3O6: Eu3+(1%) is performed using general order kinetic equation by R studio 'tgcd'. Additionally, the lifetimes of each deconvolved peaks by CGCD of Eu activated LaB3O6 (1%) have been calculated. Based on the results it can be put forth that TL characteristics of Eu doped LaB3O6 can be used as a promising material for thermoluminescence dosimetry-environmental applications.Öğe Thermoluminescence behaviour of europium doped magnesium silicate after beta exposure(Elsevier, 2020) Ucar, Z. G. Portakal; Kaynar, U. H.; Dogan, T.; Souadi, G. O.; Ayvacikli, M.; Canimoglu, A.; Topaksu, M.This article presents a detailed analysis of beta ray exposed thermoluminescence response of a series of Eu3+ doped (0.5-10 mol%) Mg2SiO4 nanocrystalline samples successfully synthesized through solid state reaction method. Optimizing the doping concentration of Eu3+ ion in Mg2SiO4 phosphor was found as 3 mol%. Two main peaks were seen at 246 degrees C and 374 degrees C and also low temperature peak at 78 degrees C. The intensities of these peaks were increased linearly with increasing beta absorbed dose. T-m-T-stop method was used to reveal trap levels. Variable heating rate and computerized glow curve deconvolution methods were also used to evaluate the number of peaks and kinetic parameters, namely activation energy and frequency factor. The results of a series of experiments carried out to investigate some fading characteristics of Mg2SiO4:Eu3+ were also presented. The findings suggest that thermoluminescence properties of Mg2SiO4:Eu(3+ )makes this material suitable and promising dosimetric phosphor material for medical applications.