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Synthesis and characteristics of N-(glyoxyldioxime)-N '-(2-hydroxybenzylidene)-1,4-diaminonaphthalene and its metal complexes
(MAIK NAUKA/INTERPERIODICA/SPRINGER, 2008) Kaya, Muharrem; Yenikaya, Cengiz; Demir, Ibrahim; Kalfa, Orhan Murat
A new vic-dioxime, N-(glyoxyldioxime)-N'-(2-hydroxybenzylidene)-1,4-diaminonaphthalene, was synthesized proceeding from naphthalene. Its complexes of nickel, copper and cobalt were prepared. The vic-dioxime and its complexes were charecterized by FT-IR, UV, H-1 NMR, mass spectrometry, elemental analysis, DTA/TG analysis techniques and conductometric measurements.
Synthesis and characterization of complexes of vic-dioxime derivatives with transition metal
(ASIAN JOURNAL OF CHEMISTRY, 2008) Kaya, Muharrem; Demir, Ibrahim; Yenikaya, Cengiz
A novel vic-dioxime compound (H(2)L) and their transition metal complexes were synthesized for the first time. This compound, N-[(4-(2,4-dihyroxybenzylideneamino)naphthalen-1-yl)]-N'-hydroxy-2-(hydroxyimino)acetimidamide, have been synthesized by starting metarial of naphthalene. The complexes of nickel(II), copper(II) and cobalt(II) with H2L were prepared. The ligand and its metal complexes were charecterized FT-IR, UV, (1)H NMR, (13)C NMR, MS, elemental analysis and conductometric measurements.