Synthesis and characterization of some vic-dioxime and its mononuclear complexes

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dc.authorid0000-0002-4763-1374
dc.contributor.authorUysal, S.
dc.contributor.authorCoskun, A.
dc.contributor.authorKoc, Z. E.
dc.contributor.authorUcan, M.
dc.contributor.authorUcan, H. I.
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued2007
dc.departmentNiğde ÖHÜ
dc.description.abstractIn this study, acetophenone is used as a basis substance. omega-Isonitrosoacetophenone has been synthesized from nitrosyl with amyl nitrite of acetophenone in the presence of sodium ethoxide. Subsequently, anti-phenylglyoxime has been prepared by reacting omega-isonitrosoacetophenone with hydroxylamine and sodium acetate in a ethanolic media. Chlorophenylglyoxime has been obtained from reaction with chlorine gases. Then, three aminophenylglyoxime (ligands) have been prepared by the reaction of chlorophenylglyoxime and the corresponding amines. The Ni(II), Co(II), and Cu(II) complexes with BF2+-bridge of anilinophenylglyoxime and 2,4-dimethylanilinophenylglyoxime were prepared. Then polymeric metal complexes with BF2+-bridge of dopamiophenylglyoxime were prepared. Their structures were identified by FT-IR, H-1 NMR, and ICP-AES spectral data, elemental analysis and magnetic measurements.
dc.identifier.doi10.1134/S1070328407050077
dc.identifier.endpage357
dc.identifier.issn1070-3284
dc.identifier.issue5
dc.identifier.scopus2-s2.0-34249693459
dc.identifier.scopusqualityQ3
dc.identifier.startpage351
dc.identifier.urihttps://dx.doi.org/10.1134/S1070328407050077
dc.identifier.urihttps://hdl.handle.net/11480/5391
dc.identifier.volume33
dc.identifier.wosWOS:000247004300007
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthor[0-Belirlenecek]
dc.language.isoen
dc.publisherMAIK NAUKA/INTERPERIODICA/SPRINGER
dc.relation.ispartofRUSSIAN JOURNAL OF COORDINATION CHEMISTRY
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.titleSynthesis and characterization of some vic-dioxime and its mononuclear complexes
dc.typeArticle

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