Micelle Mediated Extraction and Flame Atomic Absorption Spectrometric Determination of Trace Amounts of Copper in Different Mushroom Species

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dc.authoridBisgin, Abdullah Taner/0000-0002-3557-3090
dc.authoridNarin, Ibrahim/0000-0002-2275-778X
dc.contributor.authorCamci, Yeliz
dc.contributor.authorBisgin, Abdullah Taner
dc.contributor.authorSurme, Yavuz
dc.contributor.authorUcan, Mustafa
dc.contributor.authorNarin, Ibrahim
dc.date.accessioned2024-11-07T13:32:23Z
dc.date.available2024-11-07T13:32:23Z
dc.date.issued2020
dc.departmentNiğde Ömer Halisdemir Üniversitesi
dc.description.abstractA micelle mediated separation and preconcentration method for flame atomic absorption spectrophotometric (FAAS) determination of Cu was developed. The method is based on complex formation between Cu and 1-(2-pyridylazo)-2-naphthol and cloud point extraction with Tergitol NP-7 surfactant prior to FAAS determination. The parameters affecting quantitative extraction of copper, including pH, surfactant and ligand concentrations, incubation time and temperature, were examined and optimized. Under optimum conditions, interference effects of other ions were studied, and tolerance ratios of interference ions were given. Under the optimal conditions, detection and quantitation limits were found as 3 and 8 mu g/L, respectively. Linear dynamic range for Cu(2+)was determined to be 0.13-1.5 mu g/mL. Relative standard deviations were below 6% throughout the experiments. Enhancement factor was determined as 25. Applicability of the method was proved by analysis of standard reference materials. The developed method was applied to determine trace copper contents in different mushroom species.
dc.identifier.doi10.1134/S1061934820090166
dc.identifier.endpage1136
dc.identifier.issn1061-9348
dc.identifier.issn1608-3199
dc.identifier.issue9
dc.identifier.scopus2-s2.0-85090114595
dc.identifier.scopusqualityQ4
dc.identifier.startpage1131
dc.identifier.urihttps://doi.org/10.1134/S1061934820090166
dc.identifier.urihttps://hdl.handle.net/11480/15368
dc.identifier.volume75
dc.identifier.wosWOS:000565776500005
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherPleiades Publishing Inc
dc.relation.ispartofJournal of Analytical Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241106
dc.subjectcloud point extraction
dc.subject1-(2-pyridylazo)-2-naphthol (PAN)
dc.subjectcopper
dc.subjectflame atomic absorption spectrophotometry (FAAS)
dc.subjectTergitol NP-7
dc.subjectmushroom
dc.titleMicelle Mediated Extraction and Flame Atomic Absorption Spectrometric Determination of Trace Amounts of Copper in Different Mushroom Species
dc.typeArticle

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