Selective microextraction of erythrosine (E127) in foodstuffs using a new generation high-density type-V deep eutectic solvent

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dc.contributor.authorKaçanbüre, Damla
dc.contributor.authorBişgin, Abdullah Taner
dc.date.accessioned2024-11-07T10:39:38Z
dc.date.available2024-11-07T10:39:38Z
dc.date.issued2025
dc.departmentNiğde Ömer Halisdemir Üniversitesi
dc.description.abstractA novel and selective (deep eutectic solvent) DES-based microextraction method was established for the first time, utilizing a synthesized new generation High-Density Type-V DES for monitoring the dye Erythrosine (E127) in various foodstuffs and drugs. Type-V DES was created from acetophenone and diphenylamine at 3:1 M ratio. The pH, DES amount, and vortex time were optimized using Box-Behnken Design (BBD) of Response Surface Methodology (RSM). The quadratic microextraction model with R2 = 0.9982 was obtained. The limit of detection, preconcentration factor and linear dynamic range were determined to be 12 ?g/L, 50 and 41–4000 ?g/L, respectively. Effects of matrix components were examined. The developed High-Density Type-V Deep Eutectic Solvent Microextraction (HD-V-DES-ME) method was applied to foodstuffs and drugs to monitor their E127 contents and subsequently validated by applying spiked tests to real samples, with recoveries ranging between 94 and 101 %. The indexes of environmental friendliness and practicality for the method were evaluated using the Analytical GREEnness metric approach tool (AGREE) and the Blue Applicability Grade Index tool (BAGI), respectively. © 2024 Elsevier Ltd
dc.identifier.doi10.1016/j.foodchem.2024.141273
dc.identifier.issn0308-8146
dc.identifier.pmid39278080
dc.identifier.scopus2-s2.0-85203646421
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.foodchem.2024.141273
dc.identifier.urihttps://hdl.handle.net/11480/11099
dc.identifier.volume463
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoen
dc.publisherElsevier Ltd
dc.relation.ispartofFood Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241106
dc.subjectBox-Behnken design (BBD)
dc.subjectDeep eutectic solvent V (DES(V))
dc.subjectErythrosine (E127)
dc.subjectMicroextraction (ME)
dc.subjectUV–vis spectrophotometry
dc.titleSelective microextraction of erythrosine (E127) in foodstuffs using a new generation high-density type-V deep eutectic solvent
dc.typeArticle

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