Atomic absorption-spectrometric determination of copper, cadmium, lead and nickel in urine samples after enrichment and separation procedure on an activated carbon column

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dc.authorid0000-0002-1017-0244
dc.contributor.authorSoylak, M
dc.contributor.authorNarin, I
dc.contributor.authorElci, L
dc.contributor.authorDogan, M
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued1999
dc.departmentNiğde ÖHÜ
dc.description.abstractA sensitive and rapid chromatographic procedure which includes complexation of Cu, Ni, Cd and Pb with 1-(2-pyridylazo) 2-naphtol (PAN), adsorption of the metal-PAN complexes on the activated carbon column, and elution of metals with 2 M HCl in acetone, then determination of metal contents of the urine by graphite furnace atomic absorption spectrometry has been established. The influence of major components of the urine samples, as interferents, was discussed. The method has been applied for the determination of Cu, Ni, Cd and Pb in urine samples collected from inhabitants living in Nigde City of Turkey with satisfactory results such as recoveries more than 95%, relative standard deviations 2 - 6% (n = 10) and detection limits under 60 ng/l.
dc.identifier.endpage134
dc.identifier.issn0174-7371
dc.identifier.issue3
dc.identifier.scopus2-s2.0-0032790748
dc.identifier.scopusqualityN/A
dc.identifier.startpage131
dc.identifier.urihttps://hdl.handle.net/11480/5822
dc.identifier.volume16
dc.identifier.wosWOS:000081331500003
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthor[0-Belirlenecek]
dc.language.isoen
dc.publisherDUSTRI-VERLAG DR KARL FEISTLE
dc.relation.ispartofTRACE ELEMENTS AND ELECTROLYTES
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectcolumn
dc.subjectactivated carbon
dc.subjectenrichment
dc.subjectseparation
dc.subjecttrace metal
dc.subjecturine
dc.titleAtomic absorption-spectrometric determination of copper, cadmium, lead and nickel in urine samples after enrichment and separation procedure on an activated carbon column
dc.typeArticle

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