Preparation of a chelating resin by immobilizing 1-(2-pyridylazo) 2-naphtol on amberlite XAD-16 and its application ' of solid phase extraction of Ni(II), Cd(II), Co(II), Cu(II), Pb(II), and Cr(III) in natural water samples

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dc.authorid0000-0002-1017-0244
dc.contributor.authorNarin, I
dc.contributor.authorSoylak, M
dc.contributor.authorKayakirilmaz, K
dc.contributor.authorElci, L
dc.contributor.authorDogan, M
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued2003
dc.departmentNiğde ÖHÜ
dc.description.abstractA polystyrene divinylbenzene resin (Amberlite XAD-16) functionalized by 1-(2-pyridylazo) 2-naphtol has been synthesized and its sorption properties have been investigated for preconcentration of Ni(II), Cd(II), Co(II), Cu(II), Pb(II) and Cr(III) in natural water samples. The new resin (XAD-16-PAN) was characterized by thermogravimetric analysis and infrared spectrometry. The analytical parameters including pH, sample volume etc. for the quantitative recoveries of the analyte ions using XAD-16-PAN resin were investigated. The effects of alkaline, earth alkaline ions and some anions on the sorption of analyte ions were also examined. The recovery values were greater than 95% and the preconcentration factor was 200 for all analyte ions. The relative standard deviations of the determinations by flame atomic absorption spectrometry were less than 8%. The detection limits of the analyte ions (k=3, N=21) were varying from 0.056 mug/L for Cd to 0.268 mug/L for Cr.
dc.identifier.doi10.1081/AL-120018254
dc.identifier.endpage658
dc.identifier.issn0003-2719
dc.identifier.issue3
dc.identifier.scopus2-s2.0-0037245211
dc.identifier.scopusqualityQ3
dc.identifier.startpage641
dc.identifier.urihttps://dx.doi.org/10.1081/AL-120018254
dc.identifier.urihttps://hdl.handle.net/11480/5717
dc.identifier.volume36
dc.identifier.wosWOS:000181993300010
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthor[0-Belirlenecek]
dc.language.isoen
dc.publisherMARCEL DEKKER INC
dc.relation.ispartofANALYTICAL LETTERS
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectchelating resin
dc.subjectpreconcentration
dc.subjectXAD-16-PAN
dc.subjectnatural waters
dc.subjectAAS
dc.titlePreparation of a chelating resin by immobilizing 1-(2-pyridylazo) 2-naphtol on amberlite XAD-16 and its application ' of solid phase extraction of Ni(II), Cd(II), Co(II), Cu(II), Pb(II), and Cr(III) in natural water samples
dc.typeArticle

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