Determination of the effect of hydrogen peroxide on the structure of graphene produced by electrochemical method
Küçük Resim Yok
Tarih
2023
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Springer
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
It is possible to produce graphene nanosheets with the electrochemical exfoliation method. Despite the many advantages of this method, due to the nature of the process, it causes many defects in graphene. These defects, on the other hand, negatively affect the electronic properties of graphene. For this reason, in this study, a method that can reduce the destructive effects of the electrochemical method on graphene has been proposed. Herein, the electrolyte has been modified with hydrogen peroxide in the electrochemical exfoliation process, and its effect on graphene has been investigated. Structural properties, X-ray diffraction, Raman spectroscopy, energy-dispersive X-ray spectroscopy, and morphological features also were performed using scanning electron microscopy. The results were discussed by comparing them with each other and with the literature. Accordingly, it was found that when the electrolyte, which is one of the components of the electrochemical process, is modified with hydrogen peroxide, there is an effective decline in the defect density of the graphene produced. In addition, a significant decrease in the number of layers of graphene produced in the presence of hydrogen peroxide was detected.
Açıklama
Anahtar Kelimeler
Hydrogen peroxide, Nitric acid, Exfoliation graphene, Electrochemical exfoliation, Graphene nanosheet
Kaynak
Journal of Solid State Electrochemistry
WoS Q Değeri
Q3
Scopus Q Değeri
Q2
Cilt
27
Sayı
5