Polypyrrole/multi-walled carbon nanotube composite for the solid phase extraction of lead(II) in water samples

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dc.authorid0000-0002-1017-0244
dc.authorid0000-0002-7324-0385
dc.authorid0000-0001-8962-3199
dc.authorid0000-0002-4381-4456
dc.contributor.authorSahmetlioglu, Ertugrul
dc.contributor.authorYilmaz, Erkan
dc.contributor.authorAktas, Ece
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued2014
dc.departmentNiğde ÖHÜ
dc.description.abstractA multi-walled carbon nanotubes-polypyrrole conducting polymer nanocomposite has been synthesized, characterized and used for the separation and preconcentration of lead at trace levels in water samples prior to its flame atomic absorption spectrometric detection. The analytical parameters like pH, sample volume, eluent, sample flow rate that were affected the retentions of lead(II) on the new nanocomposite were optimized. Matrix effects were also investigated. Limit of detection and preconcentration factors were 1.1 mu g L-1 and 200, respectively. The adsorption capacity of the nanocomposite was 25.0 mg lead(II) per gram composite. The validation of the method was checked by using SPS-WW2 Waste water Level 2 certified reference material. The method was applied to the determination of lead in water samples with satisfactory results. (C) 2013 Elsevier B.V. All rights reserved.
dc.description.sponsorshipErciyes University; Nigde University
dc.description.sponsorshipThe authors are grateful for the financial support of the Units of the Scientific Research Project of Erciyes University and Nigde University.
dc.identifier.doi10.1016/j.talanta.2013.11.044
dc.identifier.endpage451
dc.identifier.issn0039-9140
dc.identifier.issn1873-3573
dc.identifier.pmid24401439
dc.identifier.scopus2-s2.0-84889667612
dc.identifier.scopusqualityQ1
dc.identifier.startpage447
dc.identifier.urihttps://dx.doi.org/10.1016/j.talanta.2013.11.044
dc.identifier.urihttps://hdl.handle.net/11480/4198
dc.identifier.volume119
dc.identifier.wosWOS:000331670700063
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthor[0-Belirlenecek]
dc.language.isoen
dc.publisherELSEVIER SCIENCE BV
dc.relation.ispartofTALANTA
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectConducting polymer
dc.subjectMulti-walled carbon nanotubes
dc.subjectNanocomposite
dc.subjectLead
dc.subjectSolid phase extraction
dc.titlePolypyrrole/multi-walled carbon nanotube composite for the solid phase extraction of lead(II) in water samples
dc.typeArticle

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