Separation and enrichment of chromium, copper, nickel and lead in surface seawater samples on a column filled with amberlite XAD-2000
Küçük Resim Yok
Tarih
2001
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
MARCEL DEKKER INC
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
A separation/enrichment procedure has been established for atomic absorption spectrometric determination of some trace metal ions by using a column filled Amberlite XAD-2000 resin. It is based on the sorption of metal ions on XAD-2000 as 1-(2-pyridylazo) 2-naphtol (PAN) chelates. Following washing of the XAD-2000 column with blank solution, metal-chelates were eluted by I M nitric acid in acetone and determined by flame atomic absorption spectrometry (FAAS). The influences of some analytical parameters including pH, amounts of PAN, sample volume, also effects of concomitant ions were investigated. The procedure was applied to sea water samples collected from Mersin Bay-Mediterranean Sea with satisfactory results (recoveries > 95%, relative standard deviations < 9%).
Açıklama
Anahtar Kelimeler
preconcentration, separation, metal ions, solid phase extraction, amberlite XAD-2000, seawater, AAS
Kaynak
ANALYTICAL LETTERS
WoS Q Değeri
Q3
Scopus Q Değeri
Q3
Cilt
34
Sayı
11