Cloud Point Extraction and Flame Atomic Absorption Spectrometric Determination of Cd(II) in Industrial and Environmental Samples

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dc.authoridNarin, Ibrahim/0000-0002-2275-778X
dc.authoridBisgin, Abdullah Taner/0000-0002-3557-3090
dc.contributor.authorSurme, Y.
dc.contributor.authorBisgin, A. T.
dc.contributor.authorUcan, M.
dc.contributor.authorNarin, I.
dc.date.accessioned2024-11-07T13:32:08Z
dc.date.available2024-11-07T13:32:08Z
dc.date.issued2018
dc.departmentNiğde Ömer Halisdemir Üniversitesi
dc.description.abstractA micelle-mediated separation/preconcentration technique was used for the determination of trace Cd(II) in solid and liquid samples by flame atomic absorption spectrometry. Cadmium ions reacted with ammonium pyrrolidine dithiocarbamate to form a chelate that was extracted from aqueous medium by a non-ionic surfactant Tergitol NP-7 at pH 7. Values of pH, concentrations of ammonium pyrrolidine dithiocarbamate and Tergitol NP-7, temperature, incubation time, sample volume and matrix ions were optimized. The enrichment factor of the method was found to be 25, and the detection and quantitation limits were 1.5 and 3.8 mu g/L, respectively. Assessment of the method was performed with a certified reference material, and the observed concentration of Cd(II) was in good agreement with the certified value. The method was also applied to the determination of Cd(II) in waters and industrial samples. Cd(II) concentrations in two industrial ZnO composite samples were determined between 59 and 69 mu g/g.
dc.identifier.doi10.1134/S1061934818020120
dc.identifier.endpage144
dc.identifier.issn1061-9348
dc.identifier.issn1608-3199
dc.identifier.issue2
dc.identifier.scopus2-s2.0-85051679704
dc.identifier.scopusqualityQ4
dc.identifier.startpage140
dc.identifier.urihttps://doi.org/10.1134/S1061934818020120
dc.identifier.urihttps://hdl.handle.net/11480/15245
dc.identifier.volume73
dc.identifier.wosWOS:000427389400004
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherMaik Nauka/Interperiodica/Springer
dc.relation.ispartofJournal of Analytical Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241106
dc.subjectcadmium
dc.subjectcloud point extraction
dc.subjectflame atomic absorption spectrometry
dc.subjectTergitol NP-7
dc.titleCloud Point Extraction and Flame Atomic Absorption Spectrometric Determination of Cd(II) in Industrial and Environmental Samples
dc.typeArticle

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