Qualitative and Quantitative Detection of Monofloral, Polyfloral, and Honeydew Honeys Adulteration by Employing Mid-Infrared Spectroscopy and Chemometrics

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dc.contributor.authorOzbay, Merve
dc.contributor.authorArslan, Fatma Nur
dc.contributor.authorGorur, Gazi
dc.date.accessioned2024-11-07T13:31:31Z
dc.date.available2024-11-07T13:31:31Z
dc.date.issued2022
dc.departmentNiğde Ömer Halisdemir Üniversitesi
dc.description.abstractIn this study, the potential of mid-infrared (MIR) spectroscopy complemented with chemometrics for the qualitative and quantitative detection of monofloral, polyfloral, and honeydew honeys adulteration (acacia, black cumin, carob, citrus, chestnut, lavender, linden, milk vetch, rhododendron, sunflower, thistle, thyme, honeydew, oak, and polyfloral honeys) was reported. A total of 311 honey samples (adulterated honeys with sugar syrups (2% to 50%) and pure honeys) were analyzed the spectral range of 4000-650 cm(-1). MIR data were analyzed by application of supervised and unsupervised multivariate data analyses including principle component analysis (PCA), hierarchical cluster analysis (HCA), soft independent modeling of class analogies (SIMCA), and partial least square-regression (PLS-R) analyses, by using full and characteristic wavenumber regions. The SIMCA models prescribed an excellent classification for pure honey samples of different botanical origins, and the classification limits for detecting sugar syrups added to honey samples were better than 2%. The PLS-R plots exhibited excellent predictions (R-2 > 0.9993), and the forecast calibration and validation parameters (RMSEC and RMSECV) were found as 0.4413-3.3104% and 0.6487-4.0374%, respectively. Thus, the MIR methods in conjunction with chemometrics developed here could be employed to estimate the amount of sugar syrup adulterant present at levels < 0.44% in unknown honey samples.
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [220O089]
dc.description.sponsorshipThe study was supported financially by the project from Scientific and Technological Research Council of Turkey (TUBITAK) with 220O089 number.
dc.identifier.doi10.1007/s12161-022-02266-7
dc.identifier.endpage2289
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue8
dc.identifier.scopus2-s2.0-85127973581
dc.identifier.scopusqualityQ2
dc.identifier.startpage2274
dc.identifier.urihttps://doi.org/10.1007/s12161-022-02266-7
dc.identifier.urihttps://hdl.handle.net/11480/14895
dc.identifier.volume15
dc.identifier.wosWOS:000780686100001
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofFood Analytical Methods
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241106
dc.subjectAdulteration
dc.subjectHoney
dc.subjectInfrared
dc.subjectSpectroscopy
dc.subjectChemometrics
dc.titleQualitative and Quantitative Detection of Monofloral, Polyfloral, and Honeydew Honeys Adulteration by Employing Mid-Infrared Spectroscopy and Chemometrics
dc.typeArticle

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