Ultrasound-enhanced dispersive solid phase extraction of Cd (II), Co (II), and Ni (II) using magnetic Pinus pinea

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dc.authoridKahve Yildirim, Gizem/0000-0002-3895-6812
dc.authoridSurme, Yavuz/0000-0003-4368-6658
dc.authoridNarin, Ibrahim/0000-0002-2275-778X
dc.contributor.authorSurme, Yavuz
dc.contributor.authorYildirim, Gizem Kahve
dc.contributor.authorUcan, Mustafa
dc.contributor.authorNarin, Ibrahim
dc.date.accessioned2024-11-07T13:32:23Z
dc.date.available2024-11-07T13:32:23Z
dc.date.issued2024
dc.departmentNiğde Ömer Halisdemir Üniversitesi
dc.description.abstractA new ultrasound assisted dispersive solid phase extraction (DSPE) technique has been combined with flame atomic absorption spectrometry (FAAS) to enable the simultaneous preconcentration, determination and removal of cadmium, cobalt and nickel ions from aqueous samples. In this procedure, a magnetic Pinus pinea bioadsorbent was synthesized and used as bio-adsorbent. The parameters such as solution pH, ultrasound time, analyte concentration and interfering ions were successfully optimized. All three metal ions were extracted within a mere 120 s at pH 6 and the extraction recovery values of the all three analytes were quantitative (>95%) under the optimal conditions. The adsorption processes of the metal ions were analyzed and adsorption of the metal ions were identified by Energy Dispersive X-Ray Mapping technique. A certified reference material was analyzed for the accuracy of the method. Finally, the developed method was applied for preconcentration and determination of the analytes in real water samples including natural spring water, natural mineral water and factory process water.
dc.identifier.doi10.1016/j.microc.2023.109648
dc.identifier.issn0026-265X
dc.identifier.issn1095-9149
dc.identifier.scopus2-s2.0-85178319703
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.microc.2023.109648
dc.identifier.urihttps://hdl.handle.net/11480/15364
dc.identifier.volume196
dc.identifier.wosWOS:001128349800001
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofMicrochemical Journal
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241106
dc.subjectDispersive solid phase extraction
dc.subjectUltrasound
dc.subjectPinus pinea
dc.subjectBio-adsorbent
dc.subjectFlame atomic absorption spectroscopy
dc.subjectMetal removal
dc.titleUltrasound-enhanced dispersive solid phase extraction of Cd (II), Co (II), and Ni (II) using magnetic Pinus pinea
dc.typeArticle

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