SP70-alpha-benzoin oxime chelating resin for preconcentration-separation of Pb(II), Cd(II), Co(II) and Cr(III) in environmental samples

dc.authorid0000-0002-1017-0244
dc.contributor.authorNarin, Ibrahim
dc.contributor.authorSurme, Yavuz
dc.contributor.authorBercin, Erdogan
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued2007
dc.departmentNiğde ÖHÜ
dc.description.abstractIn the presented work, a-benzoin oxime immobilized SP70 chelating resin was synthesized for separation and preconcentration of Pb(II), Cd(II), Co(II) and Cr(III). The optimization procedure for analytical parameters including pH, eluent type, flow rate, etc. was examined in order to gain quantitative recoveries of analyte ions. The effects of foreign ions on the recoveries of studied metal ions were also investigated. The detection limits Q(T) were found to be 16.0, 4.2, 1.3, 2.4 mu g L-1 for Pb, Cd, Co and Cr, respectively. The preconcentration factor was 75 for Ph, 100 for Cd, Co and Cr. The optimized method was validated with certified reference materials and successfully applied to the waters, crops and pharmaceutical samples with good results (recoveries greater than 95%, R.S.D. lower than 10%). (c) 2006 Elsevier B.V. All rights reserved.
dc.identifier.doi10.1016/j.jhazmat.2006.11.001
dc.identifier.endpage119
dc.identifier.issn0304-3894
dc.identifier.issue45323
dc.identifier.pmid17145131
dc.identifier.scopus2-s2.0-34249826966
dc.identifier.scopusqualityQ1
dc.identifier.startpage113
dc.identifier.urihttps://dx.doi.org/10.1016/j.jhazmat.2006.11.001
dc.identifier.urihttps://hdl.handle.net/11480/5375
dc.identifier.volume145
dc.identifier.wosWOS:000247702200014
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthor[0-Belirlenecek]
dc.language.isoen
dc.publisherELSEVIER SCIENCE BV
dc.relation.ispartofJOURNAL OF HAZARDOUS MATERIALS
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectchelating resin
dc.subjectsolid phase extraction
dc.subjecttrace metal
dc.subjectflame atomic absorption spectrometry
dc.titleSP70-alpha-benzoin oxime chelating resin for preconcentration-separation of Pb(II), Cd(II), Co(II) and Cr(III) in environmental samples
dc.typeArticle

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