Application of solid-phase extraction for the preconcentration and separation of trace amounts of cobalt from urine

dc.authorid0000-0002-1017-0244
dc.contributor.authorSoylak, M
dc.contributor.authorElci, L
dc.contributor.authorNarin, I
dc.contributor.authorDogan, M
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued2001
dc.departmentNiğde ÖHÜ
dc.description.abstractA solid-phase extraction method using 4-(2-thiazolylazo) resorcinol (TAR) as chelating agent on Amberlite XAD-16 column has been used for separation/preconcentration of trace amounts of cobalt prior to its determination by atomic absorption spectrometry. Cobalt was retained on the Amberlite XAD-16 column at pH 6. Cobalt was desorbed from Amberlite XAD-16 by 1 M nitric acid in acetone. The effect of the various components of urine such as some anions and cations on the recovery of cobalt was also investigated. The method was applied to urine samples collected randomly selected six people living in Kayseri with satisfactory results (recovery > 95%; relative standard deviation 1 - 9%).
dc.identifier.endpage29
dc.identifier.issn0174-7371
dc.identifier.issue1
dc.identifier.startpage26
dc.identifier.urihttps://hdl.handle.net/11480/5763
dc.identifier.volume18
dc.identifier.wosWOS:000166645200006
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.institutionauthor[0-Belirlenecek]
dc.language.isoen
dc.publisherDUSTRI-VERLAG DR KARL FEISTLE
dc.relation.ispartofTRACE ELEMENTS AND ELECTROLYTES
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjecturine
dc.subjectsolid-phase extraction
dc.subjectAmberlite
dc.subjectXAD-16
dc.subjectpreconcentration
dc.subjectcobalt
dc.titleApplication of solid-phase extraction for the preconcentration and separation of trace amounts of cobalt from urine
dc.typeArticle

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