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Öğe Synthesis and properties of N'-hydroxy-2-(hydroxyimino)-N-(4-{[(2- hydroxyphenyl)methylene]amino}-1-naphthyl)-ethanimidamide and its metal complexes(2008) Kaya M.; Yenikaya C.; Demir I.; Kalfa O.M.A new vicinal dioxime, N'-hydroxy-2-(hydroxyimino)-N-(4-{[(2-hydroxy- phenyl)methylene]amino}-1-naphthyl)ethanimidamide was synthesized. The initial compound for the synthesis of this dioxime was naphthalene. Complexes of this ligand were obtained with nickel, copper, and cobalt. The dioxime and its complexes were characterized by Fourier IR, UV, 1H NMR spectroscopy, mass spectrometry, elemental analysis, differential thermal analysis, and conductometric measurements. © 2008 MAIK Nauka.Öğe Synthesis of a imine vic-dioxime ligand and its Ni(II), Co(II), Cu(II) complexes(2008) Yenikaya C.; Kaya M.; Demir I.A novel imine vic-dioxime compound and its transition metal complexes were synthesized. The compound, N'-hydroxy-2-(hydroxyimino)-N-(4-(2,4,6- trihydro-xybenzylideneamino)-naphthalen-1-yl)acetimidamide (H2L), has been derived from naphthalene as an imine oxime ligand. The ligand and their complexes were characterized FT-IR, UV, 1H NMR, 13C NMR, MS, elemental analysis and conductometric measurements.
