Separation and determination of Pb (II) ions from aqueous media by cloud point extraction
Küçük Resim Yok
Tarih
2020
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
A simple, effective and highly selective cloud point extraction procedure was performed for enrichment of Pb (II) from aqueous matrix. The process depends on the formation of a stable complex between Pb (II) ions and Azure A compound at pH?6.0. The formed complex was extracted into micelle phase “Tergitol-NP7” at 25°C. This method was used for preconcentration of Pb (II) before its determination by FAAS. The values of limit of detection and limit of quantification were determined as 2.5 and 4.7 ?g l-1, respectively. The enrichment factor of the method was determined as 10 for 50 ml sample volume. Pb2+ analyte was quantitatively extracted and successfully determined in the presence of the most common foreign ions. The proposed method was then employed for the analysis of Pb (II) in natural and wastewater samples.
Açıklama
Anahtar Kelimeler
Kimya, Analitik, Kimya, Uygulamalı, Kimya, Tıbbi, Azure A, Cloud Point Extraction, Lead Determination, TNP7
Kaynak
International Journal of Chemistry and Technology (IJCT)
WoS Q Değeri
Scopus Q Değeri
Cilt
4
Sayı
2